Ytterbium(III) iodide explained

Ytterbium(III) iodide is one of ytterbium's iodides, with the chemical formula of YbI3.

Preparation

Ytterbium(III) iodide can be prepared by reacting metallic ytterbium with iodine at 500°C with a 30 atm pressure:[1]

2 Yb + 3 I2 → 2 YbI3

Ytterbium(III) oxide, ytterbium(III) hydroxide or ytterbium(III) carbonate can react with hydroiodic acid to obtain ytterbium(III) iodide in aqueous solution:

Yb2O3 + 6 HI → 2 YbI3 + 3 H2O

Yb(OH)3 + 3 HI → YbI3 + 3 H2O

Yb2(CO3)3 + 6 HI → 2 YbI3 + 3 H2O + 3 CO2

The ytterbium(III) iodide hydrate crystallized from the solution can be heated with ammonium iodide to obtain the anhydrous form.[2]

Reactions

Ytterbium(III) iodide decomposes to ytterbium(II) iodide upon heating:[3]

2 YbI3 → 2 YbI2 + I2

Notes and References

  1. Asprey, L. B.; Keenan, T. K.; Kruse, F. H. Preparation and crystal data for lanthanide and actinide triiodides. Inorg. Chem., 1964. 3 (8): 1137-1240
  2. 无机化学丛书 第七卷 钪 稀土元素. 科学出版社. pp 211
  3. Zeitschrift für anorganische und allgemeine Chemie. 201. 1. en. 1931-11-10. 207–220. 10.1002/zaac.19312010119. Zur Kenntnis der Halogenide der seltenen Erden. V. Über die Halogenide des Ytterbiums. 2022-09-15. G. Jantsch, N. Skalla, H. Jawurek.