Skimmianine Explained

Skimmianine is a furoquinoline alkaloid found in Skimmia japonica, a flowering plant in family Rutaceae that is native to Japan and China. It is also a strong acetylcholinesterase (AChE) inhibitor.[1]

Biosynthesis

The biosynthesis of skimmianine starts from anthranilic acid,[2] which is very abundant in the family Rutaceae. By combining anthranilic acid acetate, anthraniloyl-CoA is formed as a starting unit and able to extend side chain by adding malonyl-CoA by Claisen condensation. Next, lactam is formed through the cyclization and generate a heterocyclic system, leading the dienol tautomer adopt the 4-hydroxy quinolone tautomer, which is 4-hydroxy-2-quinolone.

With the formation of quinolone, alkylation is happening at C-3 position by introducing dimethylallyl diphosphate. Another key step is the cyclization on the dimethylallyl sidechain, forming a new heterocyclic five-member-ring.[3] Platydesmine is then forming an intermediate through the oxidative cleavage reaction[4] by losing an isopropyl group to form dictamine. Finally, skimmianine is formed through the hydroxylation of dictamine.

References

  1. 10.1007/s00044-011-9581-9 . Skimmianine, a furoquinoline alkaloid from Zanthoxylum nitidum as a potential acetylcholinesterase inhibitor . . 21 . 6 . 722–725 . 2012 . Yang . Zhong-duo . Zhang . Dong-bo . Ren . Jin . Yang . Ming-jun . 14113860 .
  2. Book: 10.1016/B978-0-12-417302-6.00009-X . Compounds Derived from Anthranilic Acid . Alkaloids . 163–180 . 2015 . 9780124173026 .
  3. Book: Manske, R. H. . 1960 . The alkaloids: Chemistry and physiology . New York . Academic Press.
  4. 10.1021/acs.chemrev.8b00031 . 6339258 . Formation and Cleavage of C–C Bonds by Enzymatic Oxidation–Reduction Reactions . Chemical Reviews . 118 . 14 . 6573–6655 . 2018 . Guengerich . F. Peter . Yoshimoto . Francis K. . 29932643 .