Nonafluoro-tert-butyl alcohol explained

Nonafluoro-tert-butyl alcohol (IUPAC name: 1,1,1,3,3,3-hexafluoro-2-(trifluoromethyl)propan-2-ol) is a fluoroalcohol. It is the perfluorinated analog of tert-butyl alcohol. Notably, as a consequence of its electron withdrawing fluorine substituents, it is very acidic for an alcohol, with a pKa value of 5.4, similar to that of a carboxylic acid. As another consequence of being a perfluorinated compound, it is also one of the lowest boiling alcohols, with a boiling point lower than that of methanol.

Synthesis

It is prepared by addition of trichloromethyllithium to hexafluoroacetone, followed by halogen exchange with antimony pentafluoride.[1] The aluminate derived from its alkoxide anion, tetrakis[1,1,1,3,3,3-hexafluoro-2-(trifluoromethyl)propan-2-oxy]aluminate(1–), is used as a weakly coordinating anion.[2]

See also

Notes and References

  1. Filler. Robert. Schure. Ralph M.. 1967-04-01. Highly acidic perhalogenated alcohols. A new synthesis of perfluoro-tert-butyl alcohol. The Journal of Organic Chemistry. EN. 32. 4. 1217–1219. 10.1021/jo01279a081. 0022-3263.
  2. Krossing. Ingo. Raabe. Ines. 2004-04-13. Noncoordinating Anions—Fact or Fiction? A Survey of Likely Candidates. Angewandte Chemie International Edition. en. 43. 16. 2066–2090. 10.1002/anie.200300620. 15083452. 1433-7851.