Chromium pentafluoride explained

Chromium pentafluoride is the inorganic compound with the chemical formula CrF5.[1] It is a red volatile solid that melts at 34 °C. It is the highest known chromium fluoride, since the hypothetical chromium hexafluoride has not yet been synthesized.[2]

Chromium pentafluoride is one of the products of the action of fluorine on a mixture of potassium and chromic chlorides.[3]

In terms of its structure, the compound is a one-dimensional coordination polymer. Each Cr(V) center has octahedral molecular geometry.[4] It has the same crystal structure as vanadium pentafluoride.[5]

Chromium pentafluoride is strongly oxidizing, able to fluorinate the noble gas xenon and oxidize dioxygen to dioxygenyl.[4] Due to this property, it decomposes readily in the presence of reducing agents, and easily hydrolyses to chromium(III) and chromium(VI).[6]

Reactions

Chromium pentafluoride can react with Lewis bases such as caesium fluoride and nitryl fluoride to give the respective hexafluorochromate(V) salt.[7]

CrF5 + CsF → CsCrF6

Chromium pentafluoride can also react with the Lewis acid antimony pentafluoride to give the CrF5·2SbF5 adduct. The adduct was found to be a strong oxidizing agent, liquid at room temperature with a melting point of −23 °C.

See also

Notes and References

  1. Book: Chromium(VI) Handbook . 2004 . CRC Press . 9780203487969 . Jacques Guertin . James A. Jacobs . Cynthia P. Avakian . 30.
  2. Riedel . Sebastian . Kaupp . Martin . 2009 . The highest oxidation states of the transition metal elements . Coordination Chemistry Reviews . 253 . 5–6 . 10.1016/j.ccr.2008.07.014 . 606–624 .
  3. Book: Fluorine Chemistry . A. G. Sharpe . J.H. Simons . Elsevier . 2012 . 24 . 9780323145435 . 2 .
  4. The structures of CrF5 and CrF5*SbF5. Shorafa, H.. Seppelt, K.. Zeitschrift für anorganische und allgemeine Chemie. 2009. 635. 1. 112–114. 10.1002/zaac.200800378.
  5. Book: Advances in Inorganic Chemistry . 27 . A. G. Sharpe . Academic Press . 1983 . 9780080578767 . 103.
  6. Book: Text Book Of Inorganic Chemistry . Amit Aora . 649 . Discovery Publishing House . 2005.
  7. Brown. S. D.. Loehr. T. M.. Gard. G. L.. 1976. The Chemistry of chromium pentafluoride II. Reaction with inorganic systems. Journal of Fluorine Chemistry. en. 7. 1. 19–32. 10.1016/S0022-1139(00)83979-2. 0022-1139.