Bis(chloromethyl) ether explained

Bis(chloromethyl) ether is an organic compound with the chemical formula (ClCH2)2O. It is a colourless liquid with an unpleasant suffocating odour and it is one of the chloroalkyl ethers. Bis(chloromethyl) ether was once produced on a large scale, but was found to be highly carcinogenic and thus such production has ceased.

Synthesis

It was produced industrially from paraformaldehyde and a mixture of chlorosulfonic acid and sulfuric acid.[1] It is also produced as a byproduct in the Blanc chloromethylation reaction, formed when formaldehyde (the monomer, paraformaldehyde or formalin) and concentrated hydrochloric acid are mixed, and is a known impurity in technical grade chloromethyl methyl ether.

Because of their carcinogenic potency, the industrial production of chloromethyl ethers ended in most countries in the early 1980s. Bis(chloromethyl) ether was no exception to this with production in the U.S.A. ending in 1982.

Uses

Bis(chloromethyl) ether has been extensively used in chemical synthesis, primarily as a crosslinking agent in the manufacture of ion-exchange resins and in the textile industry. It was also used as a linker in the synthesis of certain nerve agent antidotes (asoxime chloride, obidoxime).Bis(chloromethyl) was also effective for chloromethylation of aromatic substrates.[2]

Safety

Bis(chloromethyl) ether is carcinogenic.[3] [4] It is one of 13 chemicals considered an OSHA-regulated occupational carcinogen.[5] Chronic exposure has been linked to in increased risk of lung cancer.[3]

It is classified as an extremely hazardous substance in the United States as defined in Section 302 of the U.S. Emergency Planning and Community Right-to-Know Act (42 U.S.C. 11002), and is subject to strict reporting requirements by facilities which produce, store, or use it in significant quantities.[6]

See also

Notes and References

  1. Wilhelm Heitmann, Günther Strehlke, Dieter Mayer “Ethers, Aliphatic” Ullmann's Encyclopedia of Industrial Chemistry 2002, Wiley-VCH, Weinheim.
  2. Olah. George A.. Beal. David A.. Olah. Judith A.. Aromatic substitution. XXXVIII. Chloromethylation of benzene and alkylbenzenes with bis(chloromethyl)ether, 1,4-bis(chloromethoxy)butane, 1-chloro-4-chloromethoxybutane, and formaldehyde derivatives. The Journal of Organic Chemistry. April 1976. 41. 9. 1627–1631. 10.1021/jo00871a032.
  3. Web site: Bis(chloromethyl)ether (BCME) (CASRN 542-88-1). U.S. environmental protection agency. 26 November 2014. EPA. 2013-03-15.
  4. Van Duuren. BL. Comparison of potency of human carcinogens: vinyl chloride, chloromethylmethyl ether and bis(chloromethyl)ether.. Environmental Research. August 1989. 49. 2. 143–51. 2526731. 10.1016/s0013-9351(89)80059-3. 1989ER.....49..143V.
  5. Web site: NIOSH Pocket Guide to Chemical Hazards: bis-Chloromethyl ether. Centers for Disease Control and Prevention. 26 November 2014.
  6. Web site: . 40 C.F.R.: Appendix A to Part 355—The List of Extremely Hazardous Substances and Their Threshold Planning Quantities . July 1, 2008 . October 29, 2011 . https://web.archive.org/web/20120225051612/http://edocket.access.gpo.gov/cfr_2008/julqtr/pdf/40cfr355AppA.pdf . February 25, 2012 . dead .