2-Iminothiolane Explained

2-Iminothiolane is a cyclic thioimidate compound also known as Traut's reagent. It is a thiolating reagent that reacts with primary amine groups, such as those of amino acids, to form sulfhydryl groups.

Application

2-Iminothiolane reacts with primary amines efficiently at pH 7 to 9, creating amidine compounds with a sulfhydryl group. Thus it allows for crosslinking or labeling of molecules such as proteins through use of disulfide or thioether conjugation. It was first used to thiolate a subunit of ribosome in E. coli in 1973 by Robert Traut, its namesake, and his colleagues.[1]

It also reacts with aliphatic and phenolic hydroxyl groups at high pH, albeit at a much slower rate.[2]

References

  1. 4581787. 1973. Traut. R. R.. Methyl 4-mercaptobutyrimidate as a cleavable cross-linking reagent and its application to the Escherichia coli 30S ribosome. Biochemistry. 12. 17. 3266–73. Bollen. A. Sun. T. T.. Hershey. J. W.. Sundberg. J. Pierce. L. R.. 10.1021/bi00741a019.
  2. Web site: Traut's Reagent Instructions. Thermo Scientific. 2015-07-08.