Methcathinone Explained

Methcathinone (α-methylamino-propiophenone or ephedrone) (sometimes called "cat" or "jeff" or "catnip" or "M-Kat" or "kat" or "intash") is a monoamine alkaloid and psychoactive stimulant, a substituted cathinone. It is used as a recreational drug due to its potent stimulant and euphoric effects and is considered to be addictive, with both physical and psychological withdrawal occurring if its use is discontinued after prolonged or high-dosage administration.[1] It is usually snorted, but can be smoked, injected, or taken orally.

Methcathinone is listed as a Schedule I controlled substance by the Convention on Psychotropic Substances and the United States' Controlled Substances Act, and as such it is not considered to be safe or effective in the treatment, diagnosis, prevention, or cure of any disease, and has no approved medical use. Possession and distribution of methcathinone for the purpose of human consumption is illegal under any/all circumstances in the United States and is either illegal or highly regulated in most jurisdictions worldwide.

History

Methcathinone was first synthesized in 1928 in the United States[2] and was patented by Parke-Davis in 1957.[3] It was used in the Soviet Union during the 1930s and 1940s as an anti-depressant (under the name Эфедронephedrone). Methcathinone has long been used as a drug of abuse in the Soviet Union and Russia.

Circa 1994, the United States government recommended to the UN Secretary-General that methcathinone should be listed as a Schedule I controlled substance in the Convention on Psychotropic Substances.[4] In 1995, following US advice, China added the drug to its list of prohibited substances and discontinued its pharmaceutical use.[5]

Chemistry

Methcathinone is a beta-keto N-methylamphetamine and is closely related to the naturally occurring compounds, cathinone and cathine. It is also very closely related to methamphetamine, differing by only the β-ketone substituent and differing from amphetamine by both a keto and N-methyl substituent. Its carbon skeleton is identical to pseudoephedrine and methamphetamine. It differs from pseudoephedrine in that the hydroxide beta to the aromatic ring is oxidized to a ketone.

Methcathinone possesses a chiral carbon atom, and therefore two enantiomers are possible. When it is made semi-synthetically from pseudo/ephedrine as a starting material, then only a single enantiomer is produced. Given that the chiral center has an alpha hydrogen and adjacent the carbonyl group, the molecule will racemize in solution via an enol intermediate. This process is known as keto–enol tautomerism.

Methcathinone production utilizes the oxidation of pseudoephedrine or ephedrine, the former being preferred because of much higher yields achieved. Oxidation of pseudoephedrine to methcathinone requires little chemistry experience, making it (relatively) easy to synthesize.[6] Potassium permanganate (KMnO4) is most commonly used as the oxidant.

In clandestine laboratories, synthesizing methcathinone using potassium permanganate is considered undesirable because of the low yields and the high toxicity of this oxidant ; however, if done in a proper laboratory using the proper procedures potassium permanganate can be a high-yielding reactant. A method that yields more methcathinone is oxidizing (pseudo)ephedrine with chromium (VI) compounds.

Methcathinone as free base is very unstable; it easily loses its ketone group, which is substituted with a hydroxyl group, yielding pseudoephedrine, in the reverse of the typical synthesis reaction. Structurally, this occurs when the C=O bond at the Rβ-position is converted into a C-OH bond. Additionally, a dimerization reaction has been observed in solutions of freebase methcathinone, which yields a biologically inactive compound.[7]

Effects

Methcathinone hydrochloride increases spontaneous rodent locomotor activity,[8] potentiates the release of dopamine from dopaminergic nerve terminals in the brain, and causes appetite suppression. Users can easily forget to consume fluids leading to increased thirst and dehydration. The effects of methcathinone are similar to those of methamphetamine, initially deemed to be less intense by the inexperienced user, and often more euphoric. The effects have been compared to those of cocaine, since it commonly causes hypertension (elevated blood pressure) and tachycardia (elevated heart rate).

Reported effects include:

The effects of methcathinone usually last from four to six hours.

Pharmacology

Methcathinone has very strong affinities for the dopamine transporter and the norepinephrine (noradrenaline) transporter. Its affinity for the serotonin transporter is less than that of methamphetamine.[9]

The C=O bond at the Rβ-position (directly right of the phenyl ring) is slightly polar, and as a result the drug does not cross the lipid blood–brain barrier quite as well as amphetamine. Nevertheless, it is a potent central nervous system (CNS) stimulant and dopamine reuptake inhibitor. Chronic high dosage use may result in acute mental confusion ranging from mild paranoia to psychosis. These symptoms typically disappear quickly if use is stopped.

Anecdotal reports have provided some information on patterns of methcathinone use. The most common route of administration is via nasal insufflation (snorting). Other routes of administration include oral, IV injection and smoking.

Illicit usage

Methcathinone binges resemble amphetamine binges in that the user may not sleep or eat, and takes in little in the way of liquids. The methcathinone binge is followed by long periods of sleep, excess eating, long-lasting nosebleeds (insufflation of methcathinone is corrosive to the nasal mucosa in the same manner as methamphetamine) and, in some cases, depression.

Addiction

In preclinical studies, methcathinone hydrochloride produces an abuse potential similar to that of the amphetamines.[10]

Methcathinone can be highly psychologically addictive, and can produce a methamphetamine-like withdrawal.

In drug discrimination studies, methcathinone hydrochloride evokes responses similar to those induced by both dextroamphetamine sulfate and cocaine hydrochloride.

Intravenous usage

Injecting this substance has been associated with symptoms similar to those seen in patients with Parkinson's disease (manganism) due to the compound manganese dioxide which is a byproduct of synthesis with permanganate.[11]

Legal status

The Convention on Psychotropic Substances lists methcathinone as a Schedule I substance which restricts its use for government-approved medical and scientific uses.[12]

Australia

Methcathinone is a Schedule 9 prohibited substance in Australia under the Poisons Standard (February 2021).[13] A Schedule 9 substance is defined as a substance which may be abused or misused, the manufacture, possession, sale or use of which should be prohibited by law except when required for medical or scientific research, or for analytical, teaching or training purposes with approval of Commonwealth and/or State or Territory Health Authorities.

United Kingdom

In the United Kingdom, methcathinone is listed as a Class B drug with no clinical uses.[14]

United States

In the United States, methcathinone is listed as a Schedule I drug, for which there is no clinical use.[15]

Netherlands

In the Netherlands, methcathinone is listed as a Level I substance of the Opium Law, for which there is no clinical use.

See also

External links

Notes and References

  1. 8594170 . 27 . Journal of Psychoactive Drugs . 3 . Methcathinone: the next illicit stimulant epidemic? . 1995 . 277–85 . Calkins RF, Aktan GB, Hussain KL . 10.1080/02791072.1995.10472472.
  2. Hyde JF, Browning E, Adams R . 1928. Synthetic Homologs of d,l-Ephedrine . Journal of the American Chemical Society . 50 . 8. 2287–2292 . 10.1021/ja01395a032 .
  3. US Patent 2802865 -ETHYLAMINOPROPIOPHENONE COMPOUNDS
  4. http://www.erowid.org/chemicals/chemicals_law1.shtml Erowid
  5. News: Chinese professor accused in 'Breaking Bad' drugs plot. BBC News. 20 May 2015.
  6. https://web.archive.org/web/20131113024319/http://www.scribd.com/doc/35411/The-Clandestine-Chemists-Notebook The Clandestine Chemists Notebook
  7. 10.1093/chromsci/32.12.552. Methcathinone and Designer Analogues: Synthesis, Stereochemical Analysis, and Analytical Properties. Journal of Chromatographic Science. 32. 12. 552–564. 1994. DeRuiter J, Hayes L, Valaer A, Clark CR, Noggle FT .
  8. Glennon RA, Yousif M, Naiman N, Kalix P . Methcathinone: a new and potent amphetamine-like agent . Pharmacol. Biochem. Behav. . 26 . 3 . 547–51 . 1987 . 3575369 . 10.1016/0091-3057(87)90164-X. 5890314 .
  9. Rothman RB, Vu N, Partilla JS, Roth BL, Hufeisen SJ, Compton-Toth BA, Birkes J, Young R, Glennon RA . 6 . In vitro characterization of ephedrine-related stereoisomers at biogenic amine transporters and the receptorome reveals selective actions as norepinephrine transporter substrates . The Journal of Pharmacology and Experimental Therapeutics . 307 . 1 . 138–145 . October 2003 . 12954796 . 10.1124/jpet.103.053975 . 19015584 .
  10. 8029273 . 47 . 4 . Intravenous self-injection of methcathinone in the baboon . April 1994 . 981–3 . Kaminski BJ, Griffiths RR . Pharmacol. Biochem. Behav. . 10.1016/0091-3057(94)90307-7. 40584010 . free .
  11. De Bie RM, Gladstone RM, Strafella AP, Ko JH, Lang AE . Jun 2007 . Manganese-induced Parkinsonism associated with methcathinone (Ephedrone) abuse . Archives of Neurology . 64 . 6. 886–9 . 17562938 . 10.1001/archneur.64.6.886.
  12. Web site: Convention on Psychotropic Substances, 1971. United Nations Office on Drugs and Crime. 9 January 2013.
  13. Web site: February 2021. Poisons Standard February 2021. Therapeutic Goods Administration. Australian Government Department of Health.
  14. Web site: The Misuse of Drugs Act 1971 (Modification) Order 1998 (SI 1998 No. 750). 1998-03-18. Statutory Instrument. Ministry of Justice. 2008-07-06.
  15. Web site: Methcathinone - Partnership for Drug-Free Kids . Drugfree.org . 2015-12-23.