Iminium Explained

In organic chemistry, an iminium cation is a polyatomic ion with the general structure . They are common in synthetic chemistry and biology.

Structure

Iminium cations adopt alkene-like geometries: the central C=N unit is nearly coplanar with all four substituents. Unsymmetrical iminium cations can exist as cis and trans isomers. The C=N bonds, which are near 129 picometers in length, are shorter than C-N single bonds. Cis/trans isomers are observed. The C=N distance is slightly shorter in iminium cations than in the parent imine, and computational studies indicate that the C=N bonding is also stronger in iminium vs imine, although the C=N distance contracts only slightly. These results indicate that the barrier for rotation is higher than in the parent imines.[1] [2]

Formation

Iminium cations are obtained by protonation and alkylation of imines:

They also are generated by the condensation of secondary amines with ketones or aldehydes:

This rapid, reversible reaction is one step in "iminium catalysis".[3]

More exotic routes to iminium cations are known, e.g. from ring-opening reactions of pyridine.[4]

Occurrence

Iminium derivatives are common in biology. Pyridoxal phosphate reacts with amino acids to give iminium derivatives. Many iminium salts are encountered in synthetic organic chemistry.thumb|right|"Eschenmoser's salt" is a well known example of an iminium salt.[5]

Reactions

Iminium salts hydrolyse to give the corresponding ketone or aldehyde:[6]

Iminium cations are reduced to the amines, e.g. by sodium cyanoborohydride. Iminium cations are intermediates in the reductive amination of ketones and aldehydes.

Unsymmetrical iminium cations undergo cis-trans isomerization. The isomerization is catalyzed by nucleophiles, which add to the unsaturated carbon, breaking the C=N double bond.[1]

Named reactions involving iminium species

Iminylium ions

Iminylium ions have the general structure R2C=N+. They form a subclass of nitrenium ions.

See also

Notes and References

  1. 10.1021/jo010067k . Mechanisms of Acid-Catalyzed Z/E Isomerization of Imines . 2001 . Johnson . James E. . Morales . Nora M. . Gorczyca . Andrea M. . Dolliver . Debra D. . McAllister . Michael A. . The Journal of Organic Chemistry . 66 . 24 . 7979–7985 . 11722194 .
  2. 10.1021/jp9617332 . Factors That Influence the CN Stretching Frequency in Imines . 1997 . Wang . Youliang . Poirier . Raymond A. . The Journal of Physical Chemistry A . 101 . 5 . 907–912 . 1997JPCA..101..907W .
  3. Iminium Catalysis. Anniinä. Erkkilä. Inkeri. Majander. Petri M.. Pihko. Chem. Rev.. 2007. 107. 12. 5416–70. 10.1021/cr068388p. 18072802.
  4. Klaus. Hafner . Klaus-Peter. Meinhardt . Azulene . Organic Syntheses . 1984 . 62 . 134. 10.15227/orgsyn.062.0134.
  5. Encyclopedia: E. F. Kleinman. Dimethylmethyleneammonium Iodide and Chloride. Encyclopedia of Reagents for Organic Synthesis. 2004. J. Wiley & Sons. New York. 10.1002/047084289X.rd346.
  6. A General Synthesis of Cyclobutanones from Olefins and Tertiary Amides: 3-Hexylcyclobutanone. C. Schmit . J. B. Falmagne . J. Escudero . H. Vanlierde . L. Ghosez. Org. Synth.. 1990. 69. 199. 10.15227/orgsyn.069.0199.
  7. Grieco . P. A. . Larsen . S. D. . 1990 . Iminium Ion-Based Diels–Alder Reactions: N-Benzyl-2-Azanorborene . Organic Syntheses . 68 . 206 . 10.15227/orgsyn.068.0206.