Cerium(III) acetate explained

Cerium acetate is an inorganic compound with the chemical formula of Ce(CH3COO)3. It is a white powder that is soluble in water. Its 1.5 hydrate loses water at 133°C to obtain an amorphous anhydrous form, and the amorphous phase changes to crystal at 212°C, and phase changes again at 286°C.

Preparation

Cerium acetate can be prepared by reacting cerium(III) carbonate and 50% acetic acid in an aqueous solution:[1]

Ce2(CO3)3 + 6 CH3COOH → 2 Ce(CH3COO)3 + 3 H2O + 3 CO2

Properties

Cerium acetate is soluble in water and ethanol in its anhydrous form (its hydrate is insoluble in ethanol), easily soluble in pyridine, and insoluble in acetone.[2] Its thermal decomposition at 310 °C will generate basic cerium(III) acetate, which will be further decomposed to obtain Ce2O2CO3 (a basic carbonate), and continued heating generates CeO2 and CO.[3]

Notes and References

  1. 《无机化合物制备手册》.朱文祥 主编. 化学工业出版社.第十四章 碳族元素.P512.XIV-124 醋酸铈(III)
  2. 《无机化合物合成手册》.第二卷.日本化学会 编. 曹惠民 译. 化学工业出版社. 1988.7第一版.【1260】稀土元素的乙酸盐.P582
  3. Arii T, Kishi A, Ogawa M, et al. Thermal decomposition of cerium (III) acetate hydrate by a three-dimensional thermal analysis [J]. Analytical sciences, 2001, 17(7): 875-880.