Benzoyl chloride explained

Benzoyl chloride should not be confused with benzyl chloride.

Benzoyl chloride, also known as benzenecarbonyl chloride, is an organochlorine compound with the formula . It is a colourless, fuming liquid with an irritating odour, and consists of a benzene ring with an acyl chloride substituent. It is mainly useful for the production of peroxides but is generally useful in other areas such as in the preparation of dyes, perfumes, pharmaceuticals, and resins.

Preparation

Benzoyl chloride is produced from benzotrichloride using either water or benzoic acid:

As with other acyl chlorides, it can be generated from the parent acid and standard chlorinating agents such as phosphorus pentachloride, thionyl chloride, and oxalyl chloride. It was first prepared by treatment of benzaldehyde with chlorine.[1]

An early method for production of benzoyl chloride involved chlorination of benzyl alcohol.[2]

Reactions

It reacts with water to produce hydrochloric acid and benzoic acid:

Benzoyl chloride is a typical acyl chloride. It reacts with alcohols to give the corresponding esters. Similarly, it reacts with amines to give the amide.[3] [4]

It undergoes the Friedel-Crafts acylation with aromatic compounds to give the corresponding benzophenones and related derivatives.[5] With carbanions, it serves again as a source of the benzoyl cation synthon, .[6]

Benzoyl peroxide, a common reagent in polymer chemistry, is produced industrially by treating benzoyl chloride with hydrogen peroxide and sodium hydroxide:[7]

References

  1. 10.1002/jlac.18320030302 . Untersuchungen über das Radikal der Benzoesäure . 1832 . . 3 . 3 . 262–266 . . 2027/hvd.hxdg3f . free .
  2. https://patents.google.com/patent/US1851832 US1851832
  3. C. S.. Marvel. W. A.. Lazier. Benzoyl Piperidine. Organic Syntheses. 1929. 9. 16. 10.15227/orgsyn.009.0016.
  4. Prasenjit Saha, Md Ashif Ali, and Tharmalingam Punniyamurthy "Ligand-free Copper(ii) Oxide Nanoparticles Catalyzed Synthesis Of Substituted Benzoxazoles" Org. Synth. 2011, volume 88, pp. 398. . (an illustrative reaction of an amine with benzoyl chloride).
  5. Wesley. Minnis. 10.15227/orgsyn.012.0062. Phenyl Thienyl Ketone. Organic Syntheses. 1932. 12. 62.
  6. 10.15227/orgsyn.069.0044. Directed Reduction of a beta-keto Amide: Erythro-1-(3-hydroxy-2-methyl-3-phenylpropanoyl)piperidine. Organic Syntheses. 1990. 69. 44. M.. Fujita. T.. Hiyama.
  7. El-Samragy . Yehia . 2004 . Benzoyl Peroxide . 61st JECFA. Chemical and Technical Assessment. Joint FAO/WHO Expert Committee on Food Additives. 1. 31 October 2013. PDF. Benzoyl peroxide is synthesized commercially by the reaction of benzoyl chloride, sodium hydroxide, and hydrogen peroxide. Traces of benzoic acid remain after usual purification procedures. -->.

External links