Antimony pentasulfide explained

Antimony pentasulfide is an inorganic compound of antimony and sulfur, also known as antimony red. It is a nonstoichiometric compound with a variable composition. Its structure is unknown.[1] Commercial samples are contaminated with sulfur, which may be removed by washing with carbon disulfide in a Soxhlet extractor.

Production

Antimony pentasulfide can be produced by the reaction of antimony with sulfur at a temperature from 250 to 400 °C in an inert atmosphere.

Uses

It may be used as a red pigment and is one possible precursor to Schlippe's salt,, which can be prepared according to the equation:

It is also used in the vulcanization of rubber to produce red rubber.

Physical chemistry

Like many sulfides, this compound liberates hydrogen sulfide upon treatment with strong acids such as hydrochloric acid.[2]

Analysis by Mössbauer spectroscopy indicates that this compound is a derivative antimony(III),[3] explaining the production of antimony(III) chloride, rather than antimony(V) chloride, upon acidification. It is, therefore, not analogous to the phosphorus(V) compound phosphorus pentasulfide.

References

  1. Arnold F. Holleman, Nils Wiberg: Lehrbuch der Anorganischen Chemie, 102nd edition, de Gruyter, Berlin 2007, p. 849, .
  2. http://www.strem.com/catalog/printer.php?type=msds&catalog_number=93-5105 Strem MSDS
  3. The oxidation number of antimony in antimony pentasulfide . Inorganic and Nuclear Chemistry Letters . 5 . 1 . 1969 . 21–25 . G. G. Long . J. G. Stevens . L. H. Bowen . S. L. Ruby . 10.1016/0020-1650(69)80231-X.