Β-Propiolactone Explained

β-Propiolactone, often simply called propiolactone, is an organic compound with the formula . It is a lactone family, with a four-membered ring. It is a colorless liquid with a slightly sweet odor, highly soluble in water and organic solvents.[1] The carcinogenicity of this compound has limited its commercial applications.[2]

Production

β-Propiolactone is prepared industrially by the reaction of formaldehyde and ethenone in the presence of aluminium- or zinc chloride as catalyst:

In the research laboratory, propiolactones have been produced by the carbonylation of epoxides.[3]

Reactions and applications

It reacts with many nucleophiles in a ring-opening reactions. With water hydrolysis occurs to produce 3-hydroxypropionic acid (hydracryclic acid). Ammonia gives the β-alanine, which is a commercial process.

Propiolactone was once widely produced as an intermediate in the production of acrylic acid and its esters. That application has been largely displaced in favor of safer and less expensive alternatives. β-Propiolactone is an excellent sterilizing and sporicidal agent, but its carcinogenicity precludes that use. It is used to inactivate a wide variety of viruses,[4] for example as a step in vaccine production.[5] The principal use of propiolactone is an intermediate in the synthesis of other chemical compounds.

Safety

β-Propiolactone is "reasonably anticipated to be a human carcinogen" (IARC, 1999).[6] It is one of 13 "OSHA-regulated carcinogens," chemicals regarded occupational carcinogens by the U.S. Occupational Safety and Health Administration, despite not having an established permissible exposure limit.[7]

See also

Notes and References

  1. Merck Index, 12th Edition, entry 8005.
  2. Book: 10.1002/14356007.a15_063 . Ketenes . Ullmann's Encyclopedia of Industrial Chemistry . 2001 . Miller . Raimund . Abaecherli . Claudio . Said . Adel . Jackson . Barry . 978-3-527-30385-4 .
  3. Low Pressure Carbonylation of Epoxides to β-Lactones . John W. Kramer . Daniel S. Treitler . Geoffrey W. Coates. Org. Synth.. 2009. 86. 287. 10.15227/orgsyn.086.0287. free.
  4. 10.1111/j.1749-6632.1960.tb40931.x. Investigations of the Use of Beta-Propiolactone in Virus Inactivation. 1960. Logrippo. Gerald A.. Annals of the New York Academy of Sciences. 83. 4. 578–594. 14417982. 1960NYASA..83..578L. 6025589.
  5. Science. Development of an inactivated vaccine candidate for SARS-CoV-2. Qiang Gao . Linlin Bao . Haiyan Mao . Lin Wang . Kangwei Xu . Minnan Yang . Yajing Li . Ling Zhu . Nan Wang . Zhe Lv . Hong Gao . Xiaoqin Ge . Biao Kan . Yaling Hu . Jiangning Liu . Fang Cai . Deyu Jiang . Yanhui Yin . Chengfeng Qin . Jing Li . Xuejie Gong . Xiuyu Lou . Wen Shi . Dongdong Wu . Hengming Zhang . Lang Zhu . Wei Deng . Yurong Li . Jinxing Lu . Changgui Li . Xiangxi Wang . Weidong Yin . Yanjun Zhang . Chuan Qin . 2020-07-03. 10.1126/science.abc1932. 369. 6499. 77–81. 32376603. 7202686. 2020Sci...369...77G. free.
  6. http://ntp.niehs.nih.gov/ntp/roc/content/profiles/propiolactone.pdf "β-Propiolactone CAS No. 57-57-8"
  7. https://www.cdc.gov/niosh/npg/nengapdxb.html "Appendix B - Thirteen OSHA-Regulated Carcinogens"